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Iridium Crucible

Material: Iridium CAS# 7439-88-5

Purity: Ir>99.9%

Shapes: Cylindrical or Conical, Welded or Seamless

Size: Customized Sizes and Wall Thicknesses

Other: Refining and Supply New Crucibles with Short Lead Times

With over ten years in the industry, TFM stands out as a premier provider of high-quality Iridium Crucibles, offering competitive pricing and exceptional standards. Our experienced team excels in customizing these crucibles to meet your exact specifications, ensuring that each solution is perfectly tailored to your unique requirements.

Description

Iridium crucibles are specialized vessels for high-temperature applications, particularly metallurgy, single crystal growth, materials science, and semiconductor manufacturing. They are made from iridium, a rare and precious metal known for its exceptional properties. Iridium is the second-densest naturally occurring element, with a 22.56 g/cm³ density. It is extremely hard, brittle, and corrosion-resistant and has remarkable thermal and chemical stability, even at very high temperatures, up to 2,000°C.

Iridium crucibles are typically used for melting and holding materials at elevated temperatures in environments where other materials may degrade or react unfavorably. Due to their superior properties, iridium crucibles are ideal for handling reactive metals, alloys, and compounds that require precise control over temperature and purity during processing. Typical applications of iridium crucibles in research and development settings include crystal growth, thermal evaporation, chemical vapor deposition (CVD), and high-temperature experimentation.

Specifications of Iridium

Typical Chemical Compositions and Impurities (Ir>99.96%; ppm)

Rh42Au3Zr2
Pd22Cr3B<2
Zn21Ni3Cd<2
Pt18Os3Mn<2
Ru15Sn3As<2
Sb11Cu3Co<2
Al7Pb3Mo<2
Ca6Mg2Te<2
Se5Bi2
Si4Ag2

Electrical Properties

Electrical resistivity ( µOhmcm ): 5.1@20°C

Superconductivity critical temperature ( K ): 0.1100

Temperature coefficient ( K⁻¹ ): 0.00450 @0-100°C

Thermal emf against Pt (cold 0C – hot 100C) ( mV ): 0.65

Thermal Properties

Coefficient of thermal expansion ( x10⁻⁶ K⁻¹ ): 6.800 @0-100°C

Latent heat of evaporation ( J g⁻¹ ): 3186

Latent heat of fusion ( J g⁻¹ ): 135.00

Specific heat ( J K⁻¹ kg⁻¹ ): 133.0 @25°C

Thermal conductivity ( W m⁻¹ K⁻¹ ): 147.00 @0-100°C

Mechanical Properties

Bulk modulus ( GPa ) ( Hard / Soft ): 371.0

Hardness – Vickers ( KGF mm⁻² ) ( Hard ): 650

Hardness – Vickers ( KGF mm⁻² ) ( Soft ): 200 – 300

Material condition: Hard / Soft

Poisson’s ratio ( Hard / Soft ): 0.260

Tensile modulus ( GPa ) ( Hard / Soft ): 528.00

Tensile strength ( MPa ) ( Hard ): 1200.00

Tensile strength ( MPa ) ( Soft ): 550.00 – 1100.00

Applications of Iridium Crucible

Iridium Crucibles are crucial in various high-temperature processes, particularly in semiconductor manufacturing, materials science, and research. Some critical applications of Iridium Crucibles include:

  1. Czochralski Method (CZ Method) Crystal Growth: Iridium crucibles are primarily used in the CZ method for single crystal growth. This technique involves melting raw materials in the crucible, touching a seed crystal to the melt, and slowly rotating and pulling it up to promote crystal growth. Iridium’s high melting point and corrosion resistance make it ideal for handling this process’s extreme temperatures and chemical environments.
  2. Semiconductor Wafer Production: Iridium crucibles produce semiconductor wafers, where single crystals are grown and then sliced into thin wafers for electronic device fabrication. The high purity and stability of iridium crucibles ensure the quality and integrity of the semiconductor materials produced.
  3. LED Substrate Manufacturing: Crystals grown using iridium crucibles, such as Sapphire for LED substrates, benefit from the exceptional purity and quality achieved through the CZ method. Iridium crucibles enable the precise control of crystal growth parameters, resulting in high-quality substrates with excellent optical and electrical properties for LED applications.
  4. Optoelectronic Device Fabrication: Iridium crucibles are used to produce optoelectronic devices such as photovoltaic cells, optical filters, and laser components. Iridium’s high temperature and chemical resistance ensure the purity and uniformity of the materials used in these devices, contributing to their performance and reliability.
  5. Advanced Materials Research: In research laboratories, iridium crucibles are employed in high-temperature experiments and materials synthesis processes. Researchers use iridium crucibles to study the properties of materials at extreme conditions and develop new materials with unique characteristics for various applications.

Packaging

Our Iridium Crucibles are clearly labeled externally to ensure efficient identification and quality control. To prevent any damage during storage or transportation, we take great care.

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FAQ

A crucible is a heat-resistant container designed to hold materials during high-temperature processes such as melting, alloying, or chemical reactions. They’re essential in metal casting, laboratory analyses, and even certain thin-film deposition systems.

Crucibles are usually made from ceramics like alumina, zirconia, silicon carbide, or magnesia due to their high melting points and chemical inertness. Graphite and metal (e.g., steel) crucibles are also used for lower temperature applications.

The ideal crucible depends on the temperature and chemical nature of the process. Always select a crucible material with a melting point significantly higher than that of the material being processed and one that is chemically compatible to prevent reactions or contamination.

Always wear appropriate personal protective equipment (PPE) such as heat-resistant gloves, face shields, and aprons. Use proper tongs for handling, ensure adequate ventilation, and follow established protocols to avoid thermal shock and accidental spills.

Prior to use, crucibles are usually “dried” or pre-fired to remove moisture and avoid thermal shock. Some applications recommend a seasoning or “dressing” process to improve performance and extend the crucible’s lifespan.

Crucibles should be stored in a dry, well-ventilated area on wood shelving or other non-abrasive supports—not directly on concrete or metal floors—to avoid damage. They should also not be nested together to prevent chipping or cracking.

Yes, most crucibles are designed for multiple uses if they’re properly maintained and cleaned. However, frequent use at extreme temperatures or for reactive materials may eventually degrade them, in which case replacement is necessary.

Common challenges include cracking from rapid temperature changes (thermal shock), contamination from residual materials, and wear or erosion from high-temperature exposure. Following proper handling and maintenance guidelines helps mitigate these issues.

Allow the crucible to cool completely, then remove any residues with a suitable scraper or chemical cleaner if recommended. Some crucibles benefit from an acid wash to remove stubborn deposits—but always follow the manufacturer’s guidelines to prevent damage.

Ensure the crucible is pre-heated and free of moisture. Load the material slowly and evenly using appropriate tools to prevent splashing or uneven heating. For heavy or large pieces, use tongs or specialized equipment to maintain safety and consistency.

In metal casting, crucibles are used to melt and hold metals for forming alloys or casting components. In evaporation processes (e.g., thin-film deposition), they heat materials to their vaporization point, allowing controlled deposition onto substrates.

Their ability to withstand extreme temperatures and resist chemical reactions makes crucibles indispensable. They enable precise control over high-temperature processes in metallurgy, materials science, and chemical analysis, ensuring product quality and process reliability.

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