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Aluminum Oxide E Beam Crucibles

TFM produces high-quality aluminum oxide (Al₂O₃) E-beam crucibles, known for their excellent thermal stability and chemical resistance. These crucibles are ideal for high-temperature applications in thin-film deposition and metal evaporation, ensuring purity and precision in industries like semiconductors and optical coatings.

Introduction

Aluminum Oxide (Al₂O₃) E Beam Crucibles are high-purity ceramic containers designed for electron beam evaporation systems. In high-vacuum thin film deposition, crucible materials must withstand extreme localized heating, rapid thermal cycling, and chemical interaction with molten source materials. Alumina offers a balanced combination of thermal stability, electrical insulation, and chemical inertness, making it one of the most widely used crucible materials in E-beam evaporation.

For research laboratories and industrial coating lines alike, Aluminum Oxide E Beam Crucibles provide a dependable solution for evaporating metals, oxides, and specialty materials.

Detailed Description

Aluminum Oxide, commonly known as alumina (Al₂O₃), is a dense ceramic material characterized by high melting temperature (over 2000°C), excellent electrical insulation, and strong resistance to chemical attack. In E-beam evaporation, where the electron beam locally melts the source material, the crucible must remain dimensionally stable and resist contamination.

High-quality alumina crucibles are typically manufactured through precision ceramic forming and high-temperature sintering to achieve:

  • High purity grades (typically ≥99% Al₂O₃)

  • Dense microstructure with low open porosity

  • Smooth inner surface to reduce material trapping

  • Consistent wall thickness for uniform heat distribution

These features help maintain evaporation stability and minimize particle generation during deposition. Alumina crucibles are compatible with most standard multi-pocket copper hearth liners and can be supplied in various pocket geometries, including cylindrical, conical, and custom cavity designs.

Because alumina is electrically insulating, it prevents unintended current flow within the evaporation assembly and contributes to stable beam focusing.

Applications

Aluminum Oxide E Beam Crucibles are widely used in:

  • Metal Evaporation
    Suitable for evaporating materials such as aluminum, gold, silver, and chromium.

  • Oxide & Dielectric Deposition
    Used for evaporating oxide compounds where chemical compatibility is required.

  • Optical Coating Production
    Thin films for lenses, mirrors, and optical filters.

  • Semiconductor Fabrication
    Deposition of contact layers and dielectric films.

  • R&D Thin Film Studies
    Academic and industrial laboratories performing material development.

  • High-Vacuum Coating Systems
    Compatible with standard electron beam evaporators and multi-pocket hearths.

Technical Parameters

ParameterTypical Value / RangeImportance
Material≥99% Aluminum Oxide (Al₂O₃)Ensures chemical stability
Maximum Service Temp.>1800°C (vacuum environment)Withstands E-beam heating
Density≥3.7 g/cm³Improves structural strength
Inner DiameterCustom (e.g., 10–50 mm)Matches hearth pocket size
Wall Thickness1 – 5 mmAffects durability & heat resistance
ShapeCylindrical / Conical / CustomAdapts to source material geometry

Comparison with Related Materials

MaterialKey AdvantageTypical Application
Aluminum Oxide (Al₂O₃)Cost-effective, chemically stableGeneral metal & oxide evaporation
Boron Nitride (BN)Excellent non-wetting propertyReactive metals
GraphiteHigh thermal conductivityHigh-temperature metal evaporation
Zirconia (ZrO₂)Higher thermal shock resistanceSpecialized oxide processes

Alumina crucibles are often selected when a stable, economical, and chemically inert ceramic solution is required.

FAQ

QuestionAnswer
Can the crucible size be customized?Yes, inner diameter, height, and wall thickness can be tailored to your E-beam system.
Is alumina suitable for reactive materials?It is chemically stable for many metals and oxides; for highly reactive materials, alternative ceramics may be recommended.
What purity level is recommended?≥99% alumina is standard for vacuum evaporation to minimize contamination.
Are multi-pocket configurations supported?Yes, crucibles can be supplied to fit standard multi-pocket copper hearths.
How are they packaged?Individually packed with protective cushioning and export-grade cartons to prevent cracking during transport.

Packaging

Our Aluminum Oxide E Beam Crucibles are meticulously tagged and labeled externally to ensure efficient identification and maintain high standards of quality control. We take great care to prevent any potential damage during storage and transportation, ensuring the crucibles arrive in perfect condition.

Conclusion

Aluminum Oxide E Beam Crucibles deliver reliable performance in demanding electron beam evaporation environments. With high thermal resistance, chemical stability, and customizable geometries, they support consistent thin-film deposition across semiconductor, optical, and research applications.

For detailed specifications and a quotation, please contact us at sales@thinfilmmaterials.com.

Aluminum Oxide E Beam Crucibles

Item No.Capacities (mL)Top Diameter A (mm/inch)Height B (mm/inch)Wall Thickness C (mm/inch)Inquiry
ECAl-2217.9 (0.71″)11.8 (0.47″)2.4 (0.09″)
ECAl-3320.4 (0.81″)13.8 (0.55″)2.4 (0.09″)
ECAl-4422.5 (0.89″)15.1 (0.60″)2.4 (0.09″)
ECAl-6623.8 (0.94″)15.1 (0.59″)2.4 (0.09″)
ECAl-7729.6 (1.17″)14.3 (0.56″)2.4 (0.09″)
ECAl-7A728.6 (1.13″)13.2 (0.52″)2.4 (0.09″)
ECAl-121233.9 (1.34″)19.5 (0.77″)2.4 (0.09″)
ECAl-12A1234.3 (1.35″)17.2 (0.68″)3.2 (0.13″)
ECAl-151537.6 (1.48″)17.0 (0.67″)3.2 (0.13″)
ECAl-202042.5 (1.67″)19.5 (0.77″)2.4 (0.09″)
ECAl-252547.0 (1.85″)17.3 (0.68″)2.4 (0.09″)
ECAl-25A2541.5 (1.63″)23.9 (0.94″)2.4 (0.09″)
ECAl-303048.8 (1.92″)20.6 (0.81″)2.4 (0.09″)
ECAl-404051.6 (2.03″)25.9 (1.02″)3.2 (0.13″)
Material, shape and size can be tailored. Rectangular Aluminum crucible is available.

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FAQ

A crucible is a heat-resistant container designed to hold materials during high-temperature processes such as melting, alloying, or chemical reactions. They’re essential in metal casting, laboratory analyses, and even certain thin-film deposition systems.

Crucibles are usually made from ceramics like alumina, zirconia, silicon carbide, or magnesia due to their high melting points and chemical inertness. Graphite and metal (e.g., steel) crucibles are also used for lower temperature applications.

The ideal crucible depends on the temperature and chemical nature of the process. Always select a crucible material with a melting point significantly higher than that of the material being processed and one that is chemically compatible to prevent reactions or contamination.

Always wear appropriate personal protective equipment (PPE) such as heat-resistant gloves, face shields, and aprons. Use proper tongs for handling, ensure adequate ventilation, and follow established protocols to avoid thermal shock and accidental spills.

Prior to use, crucibles are usually “dried” or pre-fired to remove moisture and avoid thermal shock. Some applications recommend a seasoning or “dressing” process to improve performance and extend the crucible’s lifespan.

Crucibles should be stored in a dry, well-ventilated area on wood shelving or other non-abrasive supports—not directly on concrete or metal floors—to avoid damage. They should also not be nested together to prevent chipping or cracking.

Yes, most crucibles are designed for multiple uses if they’re properly maintained and cleaned. However, frequent use at extreme temperatures or for reactive materials may eventually degrade them, in which case replacement is necessary.

Common challenges include cracking from rapid temperature changes (thermal shock), contamination from residual materials, and wear or erosion from high-temperature exposure. Following proper handling and maintenance guidelines helps mitigate these issues.

Allow the crucible to cool completely, then remove any residues with a suitable scraper or chemical cleaner if recommended. Some crucibles benefit from an acid wash to remove stubborn deposits—but always follow the manufacturer’s guidelines to prevent damage.

Ensure the crucible is pre-heated and free of moisture. Load the material slowly and evenly using appropriate tools to prevent splashing or uneven heating. For heavy or large pieces, use tongs or specialized equipment to maintain safety and consistency.

In metal casting, crucibles are used to melt and hold metals for forming alloys or casting components. In evaporation processes (e.g., thin-film deposition), they heat materials to their vaporization point, allowing controlled deposition onto substrates.

Their ability to withstand extreme temperatures and resist chemical reactions makes crucibles indispensable. They enable precise control over high-temperature processes in metallurgy, materials science, and chemical analysis, ensuring product quality and process reliability.

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