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PTU0412 Low and Wide Base Platinum Crucible

Catalog No.PTU0412
Size10ml – 50ml or customized
MaterialPlatinum (Pt), PtAu5 (95% Pt and 5% Au), PtIr5 (95% Pt and 5% Ir), PtRh5 (95% Pt and 5% Rh)
PurityPt ≥ 99.95%, Ir ≥ 99.99%, Rh ≥ 99.99%, Au ≥ 99.99%

TFM provides a range of low-profile and wide-base platinum crucibles in various shapes and thicknesses. Leveraging our extensive expertise and experience in the metals sector, TFM stands out as your premier choice for high-quality crucibles.

Introduction

The Low and Wide Base Platinum Crucible is a specialized laboratory vessel designed for high-temperature chemical processing, analytical testing, and materials research. Platinum crucibles are widely recognized for their exceptional chemical inertness, high melting point, and excellent thermal stability, making them indispensable in laboratories and industrial environments where extreme conditions are required.

The low and wide base design provides improved thermal distribution and stability during heating, making this type of platinum crucible particularly suitable for gravimetric analysis, fusion processes, and high-temperature sample preparation. Its geometry allows for easier handling of samples and promotes uniform heating across the material being processed.

Detailed Description

Low and Wide Base Platinum Crucibles are manufactured from high-purity platinum, typically 99.95% Pt or higher, ensuring superior resistance to corrosion and chemical reactions. Platinum’s melting point of approximately 1768 °C allows these crucibles to operate reliably in furnaces and high-temperature analytical equipment without deformation or contamination.

The low-profile design with a wider base increases the contact area with heating surfaces, improving heat transfer efficiency and temperature uniformity. This geometry is especially beneficial for fusion reactions and analytical procedures where consistent heating is critical for achieving accurate results.

In addition to pure platinum, these crucibles may also be manufactured using platinum alloys such as Pt-Rh (Platinum-Rhodium) to enhance mechanical strength and durability at elevated temperatures. Precision forming and polishing processes ensure smooth surfaces and uniform wall thickness, reducing contamination risks and improving chemical resistance.

The wide base structure also enhances stability during heating operations, reducing the risk of tipping in laboratory furnaces or hot plates. This makes the crucible ideal for routine analytical procedures where safety and reproducibility are essential.

Applications

Low and Wide Base Platinum Crucibles are commonly used in a variety of laboratory and industrial processes, including:

  • Gravimetric chemical analysis in analytical laboratories

  • Fusion sample preparation for geological and mineral analysis

  • High-temperature reactions in materials research

  • Glass and ceramic sample melting

  • Chemical synthesis requiring inert containers

  • Quality control testing in industrial laboratories

Technical Parameters

ParameterTypical Value / RangeImportance
MaterialPlatinum (Pt) or Pt-Rh alloyProvides excellent chemical resistance
Purity≥ 99.95% PtEnsures minimal contamination
Melting Point~1768 °CSuitable for high-temperature applications
ShapeLow profile with wide baseImproves thermal distribution and stability
CapacityCustom sizes availableMatches specific laboratory needs
Surface FinishPolished interior and exteriorReduces contamination and facilitates cleaning

Comparison with Related Crucibles

MaterialKey AdvantageTypical Application
Platinum CrucibleExcellent chemical inertness and high-temperature stabilityAnalytical chemistry and fusion processes
Platinum-Rhodium CrucibleHigher mechanical strength at elevated temperaturesIntensive high-temperature laboratory work
Alumina CrucibleHigh temperature capability with lower costGeneral laboratory heating applications

FAQ

QuestionAnswer
Why choose a low and wide base crucible design?The wide base improves thermal contact and heating uniformity while providing better stability during high-temperature operations.
What purity of platinum is typically used?Most crucibles are manufactured from platinum with purity of 99.95% or higher.
Can the crucible size be customized?Yes. Capacity, dimensions, and wall thickness can be customized according to laboratory requirements.
Are platinum alloys available for increased durability?Yes. Platinum-rhodium alloys are often used to enhance mechanical strength and extend service life.
How should platinum crucibles be cleaned?They can typically be cleaned using appropriate acid solutions or high-temperature treatments depending on the contamination type.

Packaging

Our Low and Wide Base Platinum Crucibles are meticulously tagged and labeled externally to ensure efficient identification and maintain high standards of quality control. Each crucible is carefully packed in protective containers with foam cushioning and sealed packaging to prevent mechanical damage during storage and transportation.

Conclusion

The Low and Wide Base Platinum Crucible is an essential tool for high-temperature laboratory processes requiring chemical inertness, stability, and precise thermal performance. Its unique geometry improves heat distribution and operational stability, making it ideal for analytical chemistry, materials research, and industrial testing.

With high-purity platinum construction, precision manufacturing, and customizable dimensions, these crucibles provide reliable performance for demanding laboratory applications.

For detailed specifications and a quotation, please contact us at sales@thinfilmmaterials.com.

 

Low and Wide Base Platinum Crucible Specification

Size: 5ml – 125ml or customized
Material: Platinum (Pt), PtAu5 (95% Pt and 5% Au), PtIr5 (95% Pt and 5% Ir), PtRh5 (95% Pt and 5% Rh)
Purity: Pt ≥ 99.95%, Ir ≥ 99.99%, Rh ≥ 99.99%, Au ≥ 99.99%

Below is our product list, we can also provide customized low and wide base crucibles.

All weights are in grams and all dimensions are in millimeters.

Code

Description

Capacity(ml)

B

A1

Standard Weight

Reinforced base and rim Weight range

Lid Weight

PT9501

Low and wide crucible, 5ml

5

20

26

4

6

3

PT9502

Low and wide crucible, 8ml

8

21

25

6

8

3

PT9503

Low and wide crucible, 10ml

10

23

27

7

9

3

PT9504

Low and wide crucible, 10ml

10

24

29

8

13

3

PT9505

Low and wide crucible, 12ml

12

25

30

10

13

3

PT9506

Low and wide crucible, 15ml

15

27

30

11

14

3

PT9507

Low and wide crucible, 15ml

15

27

32

13

19

3

PT9508

Low and wide crucible, 20ml

20

28

33

15

18

4

PT9509

Low and wide crucible, 20ml

20

31

37

18

26

4

PT9510

Low and wide crucible, 25ml

25

30

36

19

23

4

PT9511

Low and wide crucible, 25ml

25

34

41

25

35

4

PT9512

Low and wide crucible, 30ml

30

32

40

22

27

6

PT9513

Low and wide crucible, 30ml

30

34

38

25

31

6

PT9514

Low and wide crucible, 35ml

35

33

42

25

32

6

PT9515

Low and wide crucible, 35ml

35

36

44

26

38

6

PT9516

Low and wide crucible, 40ml

40

34

43

30

36

7

PT9517

Low and wide crucible, 40ml

40

40

45

30

41

7

PT9518

Low and wide crucible, 50ml

50

42

50

36

51

8

PT9519

Low and wide crucible, 50ml

50

41

50

39

58

8

PT9520

Low and wide crucible, 60ml

60

39

48

46

54

9

PT9521

Low and wide crucible, 70ml

70

41

52

50

63

12

PT9522

Low and wide crucible, 70ml

70

45

55

53

75

12

PT9523

Low and wide crucible, 80ml

80

47

52

51

72

14

PT9524

Low and wide crucible, 90ml

90

48

57

52

81

15

PT9525

Low and wide crucible, 100ml

100

48

62

70

91

17

PT9526

Low and wide crucible, 120ml

120

57

57

84

98

22

PT9527

Low and wide crucible, 125ml

125

59

59

97

114

25

Low and Wide Base Platinum Crucible Packaging

Our Low and Wide Base Platinum Crucibles are meticulously tagged and labeled on the exterior to facilitate easy identification and ensure rigorous quality control. We prioritize safeguarding these crucibles from potential damage during both storage and transportation.

For additional support, please refer to our Platinum Maintenance Guide to help you keep your crucibles in optimal condition.

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FAQ

A crucible is a heat-resistant container designed to hold materials during high-temperature processes such as melting, alloying, or chemical reactions. They’re essential in metal casting, laboratory analyses, and even certain thin-film deposition systems.

Crucibles are usually made from ceramics like alumina, zirconia, silicon carbide, or magnesia due to their high melting points and chemical inertness. Graphite and metal (e.g., steel) crucibles are also used for lower temperature applications.

The ideal crucible depends on the temperature and chemical nature of the process. Always select a crucible material with a melting point significantly higher than that of the material being processed and one that is chemically compatible to prevent reactions or contamination.

Always wear appropriate personal protective equipment (PPE) such as heat-resistant gloves, face shields, and aprons. Use proper tongs for handling, ensure adequate ventilation, and follow established protocols to avoid thermal shock and accidental spills.

Prior to use, crucibles are usually “dried” or pre-fired to remove moisture and avoid thermal shock. Some applications recommend a seasoning or “dressing” process to improve performance and extend the crucible’s lifespan.

Crucibles should be stored in a dry, well-ventilated area on wood shelving or other non-abrasive supports—not directly on concrete or metal floors—to avoid damage. They should also not be nested together to prevent chipping or cracking.

Yes, most crucibles are designed for multiple uses if they’re properly maintained and cleaned. However, frequent use at extreme temperatures or for reactive materials may eventually degrade them, in which case replacement is necessary.

Common challenges include cracking from rapid temperature changes (thermal shock), contamination from residual materials, and wear or erosion from high-temperature exposure. Following proper handling and maintenance guidelines helps mitigate these issues.

Allow the crucible to cool completely, then remove any residues with a suitable scraper or chemical cleaner if recommended. Some crucibles benefit from an acid wash to remove stubborn deposits—but always follow the manufacturer’s guidelines to prevent damage.

Ensure the crucible is pre-heated and free of moisture. Load the material slowly and evenly using appropriate tools to prevent splashing or uneven heating. For heavy or large pieces, use tongs or specialized equipment to maintain safety and consistency.

In metal casting, crucibles are used to melt and hold metals for forming alloys or casting components. In evaporation processes (e.g., thin-film deposition), they heat materials to their vaporization point, allowing controlled deposition onto substrates.

Their ability to withstand extreme temperatures and resist chemical reactions makes crucibles indispensable. They enable precise control over high-temperature processes in metallurgy, materials science, and chemical analysis, ensuring product quality and process reliability.

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